plantbrain
Fishaholic
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You folks should not be using the KH test kits to make the Reference solution!!!
If you make a reference solution, you need to add a certain weight of chemical to a known volume of DI water(or pure solution etc).
So say adding 4.9923 grams of baking soda (heat to about 300F for 1 hour to drive off water and CO2 that accumulates in salts) to 5 liters will yield a reference solution of 40KH.
Take 10 mls of this, add 90 mls of DI water= 4 KH.
Note, you can make any number of KH references from this concentrated stock solution.
If you add a small amount of baking soda to a small volume, then the error goes way up unless you have very accurate scales and volume measurement pipettes!!!
So if you use more volume and more concentration, the errors go way down.
Then you need not be so accurate and anal.
50 liters is a bit impractical, 5 liters is not bad.
Many can get a 0.01 accuracy scale (fairly cheap), I have a 0.001 at home and 0.00001 at work.
Then you can send off a 100mls etc in a small bottle to friends etc so they can make their own.
Graduated cylinders are fairly accurate, pipettes are more so.
For each 10X magnitude dilution you increase the accuracy by 10X essentially.
There are practical considerations etc, but it's a better way to do it.
http/www.cnykoi.com/calculators/calckh.asp
Play around with this.
Try different volumes and different KH's and see how accurate the baking soda weight needs to be to achieve good accuracy.
Do not use a KH test kit which is not calibrated to make a solution.
You compare the reference solution to the KH test kit, not the other way around!!!!!
Here's more on dilutions so you can make whatever KH reference solution once you make the stock solution:
For diutions:
http/www.wellesley.edu/Biology/Concepts/...metovolume.html
This should get more of you off the duff and try this method out and see it's not hard and it's a lot more accurate. Many look and see, but need it laid out to actually try it.
So both methods avoid chemical stuff that scares you most, and all you do is add baking soda. DI water and make a drop checker of wrap the pH probe etc in a DO membrane and KH ref solution.
From here you have a very accurate method to measure CO2.
Regards,
Tom Barr
If you make a reference solution, you need to add a certain weight of chemical to a known volume of DI water(or pure solution etc).
So say adding 4.9923 grams of baking soda (heat to about 300F for 1 hour to drive off water and CO2 that accumulates in salts) to 5 liters will yield a reference solution of 40KH.
Take 10 mls of this, add 90 mls of DI water= 4 KH.
Note, you can make any number of KH references from this concentrated stock solution.
If you add a small amount of baking soda to a small volume, then the error goes way up unless you have very accurate scales and volume measurement pipettes!!!
So if you use more volume and more concentration, the errors go way down.
Then you need not be so accurate and anal.
50 liters is a bit impractical, 5 liters is not bad.
Many can get a 0.01 accuracy scale (fairly cheap), I have a 0.001 at home and 0.00001 at work.
Then you can send off a 100mls etc in a small bottle to friends etc so they can make their own.
Graduated cylinders are fairly accurate, pipettes are more so.
For each 10X magnitude dilution you increase the accuracy by 10X essentially.
There are practical considerations etc, but it's a better way to do it.
http/www.cnykoi.com/calculators/calckh.asp
Play around with this.
Try different volumes and different KH's and see how accurate the baking soda weight needs to be to achieve good accuracy.
Do not use a KH test kit which is not calibrated to make a solution.
You compare the reference solution to the KH test kit, not the other way around!!!!!
Here's more on dilutions so you can make whatever KH reference solution once you make the stock solution:
For diutions:
http/www.wellesley.edu/Biology/Concepts/...metovolume.html
This should get more of you off the duff and try this method out and see it's not hard and it's a lot more accurate. Many look and see, but need it laid out to actually try it.
So both methods avoid chemical stuff that scares you most, and all you do is add baking soda. DI water and make a drop checker of wrap the pH probe etc in a DO membrane and KH ref solution.
From here you have a very accurate method to measure CO2.
Regards,
Tom Barr