what size bottle and what is your mix ratio? When i had DIY co2 in a planted tank (yes Liz, Ive been a very green girl before

) Id use a 16-20 oz soda bottle and mix a teaspoon of yeast to 1/8 cup sugar with about 1/8th tspoon baking soda as a buffer.
put the sugar and baking soda in the bottle, dissolve with hot water from the tap (will be cool enough for the yeasties by the time the sugar dissolves), shake vigorously until dissolved,then add the yeast. shake gently and hook it up to the tank. I always had 2 bottles running at any given time joined by a gang valve. Would remix each once a week on alternate days (one like wed and one say sat)..that way you are never really "out" of co2.
this system worked great for me. constant steady co2 and no algae. the most difficult part of the entire assembly was making sure the cap of the bottle was very well sealed with the tubing..i think i used superglue to seal around it but dont really remember. also make sure the bottles are kept somewhat warm. cold water=cold yeast and slow produced co2. The age of the yeast is also important so if it had been sitting around for a while (a few months in the fridge for example) might be time to get new yeast. equally important is to keep the yeast that you intend to use IN the fridge and not on a shelp somewhere. keeps it "dormant" until ready to mix.
hope that helped. feel free to ask questions and ill do my best to jog my memory lol
cheers